25-30 August 2019
Henry Ford Building
Europe/Berlin timezone

Multiple acquisitions for protein assignment, structure and dynamics

29 Aug 2019, 11:55
Lecture Hall D (Henry Ford Building)

Lecture Hall D

Henry Ford Building

Invited talk Solid-state NMR development and applications Solid-state NMR Methods


Prof. Józef Lewandowski (University of Warwick)


In this presentation I will discuss various implementations of multiple detection experiments for accelerating assignment, structure determination and relaxation measurements in the solid state NMR. Methods will include multiple receiver variants of time-shared TSAR experiments for obtaining long distance restraints, 1H-detected and 13C-detected experiments for spectral assignment compensated for the lower sensitivity of 13C detection and various implementations of sequential experiments for measuring simultaneously 15N and 13C' R1 and R. Various experimental consideration for multiple detection experiments will be discussed.

Primary authors

Trent Franks (University of Warw) Angelo Gallo (University of Warwick-Department of Chemistry) Ms Jacqueline Tognetti (University of Warwick) Prof. Józef Lewandowski (University of Warwick)

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